By H. Fischer (auth.), H. Fischer (eds.)
Volume II/26 supplementations the former compilations II/l, II/9 and II/17 of the magnetic homes of unfastened radicals. end result of the nonetheless speedy development of the sphere and the mandatory inclusion of recent matters the amount is split into subvolumes with the intention to seem in quickly succession. including the sooner courses quantity II/26 deals an up to date and accomplished survey and number of buildings and information at the vital chemical intermediates, specifically radicals, polyradicals and comparable species comparable to carbenes. As earlier than the species were grouped based on chemical points. for every workforce of drugs the literature has been compiled and extracted by means of specialists within the fields. For the readers comfort an index of drugs follows within the final subvolume.
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Extra info for Conjugated Carbon Centered Radicals, High-Spin System and Carbenes
32 97Bel1/ 94Cor1/ 96Shc1 CF2CF3 2 F3C 1 . 2 Cyclopentenyl radicals Co g-irr. of cyclopentene at 77 K and annealing to 150 K 60 [C5H7] 2 . 1 5 3 CCl3F 4 ESR / 77 Co g-irr. of cyclopentene at 77 K 60 CCl2FCClF2 ESR / 97 INDO, AM1 calculations. 40 93Bar1/ 94Cro11) ESR / 133 Co g-irr. of norbornadiene or quadricyclane adsorbed in zeolite at 77 K 60 ESR / 260 1) MNDO, AM1, PM3 calculations. Landolt-Bö rnstein New S eries II/ 26B 5 Carbon radicals with conjugated p-systems Ref. p. 303] 47 Substance Generation / Matrix or g-Factor / Solvent / Method / T [K] a-Value [mT] Ref.
C6H6Cl2F6NOSi] Add. of ◊SiCl(CH3)2 to corresp. 49(1)1) 91Hol2/ 87Clo1/ 93Clo1 . Cl CF3 1C N C3 OSiCl(CH3)2 F3C Toluene ESR / 203 [C8H6Cl2F10NOSi] . Cl CF3 1C N C3 OSiCl(CH3)2 F3CF2CF2C Add. of ◊SiCl(CH3)2 to corresp. imidoyl chloride Toluene ESR / 293 [C5H7N5O2]+ O H N H2N X-irr. of guanine·HBr· H2O at 8 or 65 K H . N+CHOH N [C9H11NO2S]+ CH3 NH Single crystal (monoclinic, P21/c) ESR, ENDOR, EIE / 65 1) Not exchanged in partially deuterated guanine. γ-irr. 9 89Rho2 ESR / 77 . H SO2 N+ H 2 1 H 3 H Co g-irr.
C9HF16O] . F3C 1 Photored. of (F3C)2C= C[CF(CF3)2]COCF3 CF(CF3)2 CF3 2 CF3 OH [C10F19O] . F3C 1 [C15H15F16OSi] . 35(1) 98Bai1 Neat 3 CF3 OCF3 F3C 89Tum1 ESR / 293 Phot. 076 3 CF3 OSi(CH2CH3)3 ESR / 293 Phot. of DTBP in the presence of triethylsilane and (F3C)2C= C[CF(CF3)2]COCF3 DTBP ESR / 293 [C3H5O2] . HO 1 X-irr. 2 Substituted allyl radicals 34 Substance Generation / Matrix or g-Factor / Solvent / Method / T [K] a-Value [mT] [C3H5O2] (continued) Reaction of HO◊ (TiIIIH2O2) with fumaric acid [C4H5O4] .
Conjugated Carbon Centered Radicals, High-Spin System and Carbenes by H. Fischer (auth.), H. Fischer (eds.)